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341350A-EN V1.2 1/14
7
pHTroubleshootingChart
Symptom Cause RecommendedSolution
Longresponse
timeorreading
drift
CloggedJunction Soakin4.07MKCL@60
o
Cfor30
minutes
Oil,paint,dyes,suspendedsolidson
sensor
Rinseelectrodealternatelywith
materialssolventthenbuffer7.00
DryBulb Longtermstoragewithoutwetting Soakelectrodetipinwettingcapfilled
with1ml7.00bufferfor24to48hours
StaticCharge Wipingelectrodes Rinseelectrodein7.0bufferandblot.
Donowipeelectrode.
Samereadingsin
differentbuffers
andsamples
Crackedorbrokenbulb Replaceelectrode.Usebulbguard.
Avoidplungingelectrodetobottomof
containerandspinningbars.Awetting
capwillprotectbulbbetween
measurements.
ErraticLCD
display
Sampleshavelowionicstrength
(lackssalt);e.g.distilled,deionized,
boiled,lakewater(highpressure)
Foreach50mlofsampleadd1drop
(50uL)ofSAT.KCLNoalterationinpH
willoccurbyinertKCL.
NotesonpHmeasurementsandelectrodes
1. TheElectrodeshouldbestoredinitswettingcapuntilused.UseapH4buffersolutionor
tapwaterasthestoragemedium.
2. Ifbubblesareseeninthebulbarea,holdtheelectrodebyitscapandshakedownwards
untilbubblesareremoved.
3. Toimprovespeedofresponse,vigorouslystirtheelectrodeinthesample,buffer,orrinse
solution.
4. Afterexposuretoasample,buffer,orrinsesolution,shaketheelectrodewithasnap
motiontoremoveresidualdropsofsolution.
5. Whenpossible,usepartofthenextsample/buffertobemeasuredasarinsesolution,.
6. Keepbuffersandsamplesatthesametemperaturetoavoidtemperatureeffects.
7. pHreadingsstabilizefasterinsomesolutionsthanothers;allowtimetostabilize.
8. Electrodesdeteriorateovertime.Ifaccuracyfallsto10%theelectrodeshouldbecleaned.If
noimprovementisobserved,replacetheelectrode.
NotesontheConductivity/TDS/SaltCell
1. CellStorage:Onsheathedcells,replacethesheathoverthecellwhenstoring.Fornon
sheathedversions,soakthecelltipindeionizedwaterforstorage.
2. CellCleaning:Aftereachuse,thecelltipshouldberinsedwithdeionizedwater.Ifsolids
buildupinsidethecellcarefullyremovewithacottonswabsoakedinsolventtakingcare
nottotouchthemetalpartsoftheinnercell.